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The changes in internal structure have been observed by means of the scanning electron microscope and the mercury porosimeter.
The procedure for obtaining volume-change behavior under isotropic conditions for a large range of pressures using the mercury porosimeter is also presented for oven-dried samples.
A mercury porosimeter is an instrument that allows the total volume of a powder to be determined, as well as the volume of pores of different sizes: A known mass of powder is submerged in mercury.
