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Ethanol (40 mL) was cautiously added dropwise, followed by the dropwise addition of 200 mL of water.
A common procedure includes the dropwise addition of concentrated sulfuric acid to a cooled mixture of an aqueous sodium nitrite solution and an alcohol.
Dropwise addition of calcium acetate solution into a sodium acid phosphate solution at pH 5 or 6, maintained at 60 C for 3 to 4 hours.
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